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CH420-15 Analytical Frontiers in a Changing World

Department
Chemistry
Level
Undergraduate Level 4
Module leader
Mark Barrow
Credit value
15
Module duration
10 weeks
Assessment
20% coursework, 80% exam
Study location
University of Warwick main campus, Coventry

Introductory description

The module provides a focus upon advanced aspects of analytical science, building upon core concepts of analytical science covered in Year 1 and Year 2 modules. The Year 3 module “CH3H1: Analytical Science and Global Challenges” offers useful background but is not a prerequisite. The lectures will each have a theme, where they present students with a question at the beginning, which the material then addresses. Solid state nuclear magnetic resonance (NMR) will be introduced, building upon Year 2 coverage of solution phase NMR. Electron paramagnetic resonance (EPR) spectroscopy, not previously covered during the course, will be introduced and the module will cover more sophisticated experimental designs and strategies for data analysis. The lectures will be supported by case studies to link understanding of theory with real world applications. In particular, there will be a focus on how analytical science directly guides advances in sustainability, such as understanding the environmental impact of anthropogenic activities and development of future materials and sources of energy.

Module web page

Module aims

Students will learn how advances in analytical science directly guide advances in the modern world, particularly with respect to energy, health, and the environment. They will be trained in analysis and interpretation of data encompassing mass spectrometry, EPR, and solid-state NMR. They will learn how to plan experiments and analyse and interpret data

Outline syllabus

This is an indicative module outline only to give an indication of the sort of topics that may be covered. Actual sessions held may differ.

The module is divided into three areas of modern analytical instrumentation:
(1) Mass spectrometry: introductions/basics, hyphenation (coupling with complementary techniques), interpretation of data, and AI
(2) Electron paramagnetic resonance: introduction, interpretation of data, reaction monitoring, advanced EPR techniques/applications.
(3) Nuclear magnetic resonance: solid state NMR, vector model and pulse sequences, , relaxation, exchange, double resonance experiments, and dynamic nuclear polarisation

Learning outcomes

By the end of the module, students should be able to:

  • Understand the principles and capabilities of advanced analytical techniques: mass spectrometry, electron paramagnetic resonance spectroscopy, and solid-state NMR spectroscopy.
  • Understand and explain strategies for data analysis
  • Discuss roles of analytical science plays towards developments in the modern world, including energy, the environment, and health care, amongst others.
  • Analyse and interpret real-world analytical data

Indicative reading list

Reading lists can be found in Talis

Specific reading list for the module

Subject specific skills

Atomic and Molecular Structure
Spectroscopy and Structural Characterisation
Sustainability and Green Chemistry

Transferable skills

Critical thinking
Problem solving   
Digital literacy

Study time

Type Required
Lectures 16 sessions of 1 hour (11%)
Practical classes 3 sessions of 1 hour (2%)
Other activity 1 hour (1%)
Private study 130 hours (87%)
Total 150 hours

Private study description

N/A

Other activity description

Lab tour of analytical facilities (mass spectrometry, NMR, and EPR) at Millburn House

Costs

No further costs have been identified for this module.

You do not need to pass all assessment components to pass the module.

Assessment group D
Weighting Study time Eligible for self-certification
Assessment component
Problem sets 20% Yes (extension)

Three, short assessments on the topics of mass spectrometry, EPR, and NMR experiments and data analysis.

Reassessment component is the same
Assessment component
Written examination 80% No
  • Answerbook Pink (12 page)
  • Students may use a calculator
  • Periodic Tables
Reassessment component is the same
Feedback on assessment

Individual feedback provided to students via Moodle/Tabula

Past exam papers for CH420

Courses

This module is Optional for:

  • UCHA-F110 Undergraduate Master of Chemistry (with Industrial Placement)
    • Year 4 of F110 MChem Chemistry (with Industrial Placement)
    • Year 4 of F112 MChem Chemistry with Medicinal Chemistry with Industrial Placement
  • Year 5 of UCHA-F107 Undergraduate Master of Chemistry (with Intercalated Year)
  • UCHA-F109 Undergraduate Master of Chemistry (with International Placement)
    • Year 4 of F109 MChem Chemistry (with International Placement)
    • Year 4 of F111 MChem Chemistry with Medicinal Chemistry (with International Placement)
  • UCHA-4M Undergraduate Master of Chemistry Variants
    • Year 4 of F105 Chemistry
    • Year 4 of F110 MChem Chemistry (with Industrial Placement)
    • Year 4 of F109 MChem Chemistry (with International Placement)
    • Year 4 of F125 MChem Chemistry with Medicinal Chemistry
  • Year 5 of UCHA-F127 Undergraduate Master of Chemistry with Medicinal Chemistry(with Intercalated Year)