CH420-15 Analytical Frontiers in a Changing World
Introductory description
The module provides a focus upon advanced aspects of analytical science, building upon core concepts of analytical science covered in Year 1 and Year 2 modules. The Year 3 module “CH3H1: Analytical Science and Global Challenges” offers useful background but is not a prerequisite. The lectures will each have a theme, where they present students with a question at the beginning, which the material then addresses. Solid state nuclear magnetic resonance (NMR) will be introduced, building upon Year 2 coverage of solution phase NMR. Electron paramagnetic resonance (EPR) spectroscopy, not previously covered during the course, will be introduced and the module will cover more sophisticated experimental designs and strategies for data analysis. The lectures will be supported by case studies to link understanding of theory with real world applications. In particular, there will be a focus on how analytical science directly guides advances in sustainability, such as understanding the environmental impact of anthropogenic activities and development of future materials and sources of energy.
Module aims
Students will learn how advances in analytical science directly guide advances in the modern world, particularly with respect to energy, health, and the environment. They will be trained in analysis and interpretation of data encompassing mass spectrometry, EPR, and solid-state NMR. They will learn how to plan experiments and analyse and interpret data
Outline syllabus
This is an indicative module outline only to give an indication of the sort of topics that may be covered. Actual sessions held may differ.
The module is divided into three areas of modern analytical instrumentation:
(1) Mass spectrometry: introductions/basics, hyphenation (coupling with complementary techniques), interpretation of data, and AI
(2) Electron paramagnetic resonance: introduction, interpretation of data, reaction monitoring, advanced EPR techniques/applications.
(3) Nuclear magnetic resonance: solid state NMR, vector model and pulse sequences, , relaxation, exchange, double resonance experiments, and dynamic nuclear polarisation
Learning outcomes
By the end of the module, students should be able to:
- Understand the principles and capabilities of advanced analytical techniques: mass spectrometry, electron paramagnetic resonance spectroscopy, and solid-state NMR spectroscopy.
- Understand and explain strategies for data analysis
- Discuss roles of analytical science plays towards developments in the modern world, including energy, the environment, and health care, amongst others.
- Analyse and interpret real-world analytical data
Indicative reading list
Reading lists can be found in Talis
Specific reading list for the module
Subject specific skills
Atomic and Molecular Structure
Spectroscopy and Structural Characterisation
Sustainability and Green Chemistry
Transferable skills
Critical thinking
Problem solving
Digital literacy
Study time
| Type | Required |
|---|---|
| Lectures | 16 sessions of 1 hour (11%) |
| Practical classes | 3 sessions of 1 hour (2%) |
| Other activity | 1 hour (1%) |
| Private study | 130 hours (87%) |
| Total | 150 hours |
Private study description
N/A
Other activity description
Lab tour of analytical facilities (mass spectrometry, NMR, and EPR) at Millburn House
Costs
No further costs have been identified for this module.
You do not need to pass all assessment components to pass the module.
Assessment group D
| Weighting | Study time | Eligible for self-certification | |
|---|---|---|---|
Assessment component |
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| Problem sets | 20% | Yes (extension) | |
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Three, short assessments on the topics of mass spectrometry, EPR, and NMR experiments and data analysis. |
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Reassessment component is the same |
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Assessment component |
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| Written examination | 80% | No | |
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Reassessment component is the same |
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Feedback on assessment
Individual feedback provided to students via Moodle/Tabula
Courses
This module is Optional for:
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UCHA-F110 Undergraduate Master of Chemistry (with Industrial Placement)
- Year 4 of F110 MChem Chemistry (with Industrial Placement)
- Year 4 of F112 MChem Chemistry with Medicinal Chemistry with Industrial Placement
- Year 5 of UCHA-F107 Undergraduate Master of Chemistry (with Intercalated Year)
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UCHA-F109 Undergraduate Master of Chemistry (with International Placement)
- Year 4 of F109 MChem Chemistry (with International Placement)
- Year 4 of F111 MChem Chemistry with Medicinal Chemistry (with International Placement)
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UCHA-4M Undergraduate Master of Chemistry Variants
- Year 4 of F105 Chemistry
- Year 4 of F110 MChem Chemistry (with Industrial Placement)
- Year 4 of F109 MChem Chemistry (with International Placement)
- Year 4 of F125 MChem Chemistry with Medicinal Chemistry
- Year 5 of UCHA-F127 Undergraduate Master of Chemistry with Medicinal Chemistry(with Intercalated Year)